manifestation_id original_title title_alternative title_transcription statement_of_responsibility manifestation_identifier creator contributor publisher date_of_publication pub_date year_of_publication publication_place manifestation_created_at manifestation_updated_at carrier_type content_type frequency language isbn issn doi jpno ncid lccn iss_itemno volume_number volume_number_string edition edition_string issue_number issue_number_string serial_number extent start_page end_page dimensions height width depth manifestation_price access_address manifestation_required_role abstract description identifier:unknown identifier:nbn identifier:isbn10 identifier:iss_itemno identifier:online_isbn identifier:print_isbn identifier:print_issn identifier:online_issn identifier:escidoc identifier:nims series_statement_id series_statement_original_title series_statement_title_subseries series_statement_title_subseries_transcription series_statement_title_transcription series_statement_creator series_statement_volume_number series_statement_series_master series_statement_root_manifestation_id series_statement_manifestation_id series_statement_position series_statement_note series_statement_created_at series_statement_updated_at subject:ndlsh subject:unknown subject:bsh classification:ndc8 classification:ndc9 classification:udc item_id item_identifier binding_item_identifier call_number library shelf item_note accepted_at acquired_at item_created_at item_updated_at 105465 "Everything SAXS: Small-angle scattering pattern collection and correction" "" "" "" 2015-12-15 21:32:09 +0900 2025-07-14 15:47:34 +0900 online_resource text unknown unknown "" "" https://hdl.handle.net/20.500.11932/1758193 Guest " For obtaining reliable nanostructural details of large amounts of sample --- and if it is applicable --- Small-Angle Scattering (SAS) is a prime technique to use. It promises to obtain bulk-scale, statistically sound information on the morphological details of the nanostructure, and has thus led to many a researcher investing their time in it over the last eight decades of development. Due to pressure both from scientists requesting more details on increasingly complex nanostructures, as well as the ever improving instrumentation leaving less margin for ambiguity, small-angle scattering methodologies have been evolving at a high pace over the last few decades. As the quality of any results can only be as good as the data that goes into these methodologies, the improvements in data collection and all imaginable data correction steps are reviewed here. This work is intended to provide a comprehensive overview of all data corrections, to aid the small-angle scatterer to decide which are relevant for their measurement and how these corrections are performed. Clear mathematical descriptions of the corrections are provided where feasible. Furthermore, as no quality data exists without a decent estimate of its precision, the error estimation and propagation through all these steps is provided alongside the corrections. With these data corrections, the collected small-angle scattering pattern can be made of the highest standard allowing for authoritative nanostructural characterisation through its analysis. A brief background of small-angle scattering, the instrumentation developments over the years, and pitfalls that may be encountered upon data interpretations are provided as well. " "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" Condensed Matter//Materials Science//cond-mat.mtrl-sci//Physics//Data Analysis//Statistics and Probability//physics.data-an//Physics//Instrumentation and Detectors//physics.ins-det//Condensed Matter//Materials Science//cond-mat.mtrl-sci//Physics//Data Analysis//Statistics and Probability//physics.data-an//Physics//Instrumentation and Detectors//physics.ins-det//Condensed Matter//Materials Science//cond-mat.mtrl-sci//Physics//Data Analysis//Statistics and Probability//physics.data-an//Physics//Instrumentation and Detectors//physics.ins-det//Condensed Matter//Materials Science//cond-mat.mtrl-sci//Physics//Data Analysis//Statistics and Probability//physics.data-an//Physics//Instrumentation and Detectors//physics.ins-det "" "" "" "" 104484 web web 2025-07-14 15:02:36 +0900 2025-07-14 15:47:34 +0900 105464 ORCID Ninja Tokyo 2014 Tanabe, Kosuke//TANIFUJI Mikiko "" "" 2015-12-15 21:32:08 +0900 2025-07-14 15:47:34 +0900 online_resource text unknown unknown "" "" https://hdl.handle.net/20.500.11932/1758195 Guest "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" Ninja//Samurai//ORCID//Ninja//Samurai//ORCID//Ninja//Samurai//ORCID//Ninja//Samurai//ORCID "" "" "" "" 104483 web web 2025-07-14 15:02:35 +0900 2025-07-14 15:47:34 +0900 105461 ORCID Ninja Tokyo 2014 Tanabe, Kosuke//TANIFUJI Mikiko "" "" 2015-12-15 21:32:03 +0900 2025-07-14 15:47:34 +0900 online_resource text unknown unknown "" "" https://hdl.handle.net/20.500.11932/1758189 Guest "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" talk//ORCID//Ninja//Samurai//talk//ORCID//Ninja//Samurai//talk//ORCID//Ninja//Samurai//talk//ORCID//Ninja//Samurai "" "" "" "" 104480 web web 2025-07-14 15:02:35 +0900 2025-07-14 15:47:34 +0900 105440 表面科学分野における放射光結晶学(入門講座) "" "" "" 2005-01-01 00:00:00 +0900 2005 2005 2015-12-15 21:31:33 +0900 2025-07-14 15:47:31 +0900 online_resource text unknown unknown "" "" 371 379 https://hdl.handle.net/20.500.11932/1613634 Guest "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" 104459 web web 2025-07-14 15:02:33 +0900 2025-07-14 15:47:31 +0900 105439 X線逆格子イメージング法によるナノ材料の迅速評価 坂田, 修身//吉本, 護//三木, 一司 "" "" 2006-01-01 00:00:00 +0900 2006 2006 2015-12-15 21:31:31 +0900 2025-07-14 15:47:31 +0900 online_resource text unknown unknown "" "" 992 997 https://hdl.handle.net/20.500.11932/1613633 Guest "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" 104458 web web 2025-07-14 15:02:32 +0900 2025-07-14 15:47:31 +0900 105438 酸素吸着によるRu表面の多層乱れーナノ微粒子の実験的シミュレーション 中村, 将志//加藤, 勇人//星, 永宏//隅谷, 和嗣//坂田, 修身 "" "" 2007-01-01 00:00:00 +0900 2007 2007 2015-12-15 21:31:28 +0900 2025-07-14 15:47:31 +0900 online_resource text unknown unknown "" "" 86 89 https://hdl.handle.net/20.500.11932/1613631 Guest "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" 104457 web web 2025-07-14 15:02:32 +0900 2025-07-14 15:47:31 +0900 105437 X線回折法によるナノ材料の界面構造の迅速評価 坂田, 修身//吉本, 護//三木, 一司 "" "" 2007-01-01 00:00:00 +0900 2007 2007 2015-12-15 21:31:27 +0900 2025-07-14 15:47:31 +0900 online_resource text unknown unknown "" "" 49 52 https://hdl.handle.net/20.500.11932/1613610 Guest "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" 104456 web web 2025-07-14 15:02:32 +0900 2025-07-14 15:47:31 +0900 105436 高輝度放射光X線回折法を用いたナノ構造解析の最近の話題 "" "" "" 2009-03-01 00:00:00 +0900 2009-03-01 2009 2015-12-15 21:31:22 +0900 2025-07-14 15:47:31 +0900 online_resource text unknown unknown "" "" 79 85 https://hdl.handle.net/20.500.11932/1613604 Guest "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" 104455 web web 2025-07-14 15:02:32 +0900 2025-07-14 15:47:31 +0900 105319 Effect of substitution of 3d metals for Cu in Bi2(Sr0.6Ca0.4)3Cu2Oy "" "" "" 2002-11-20 00:00:00 +0900 2002-11-20 2002 2015-12-15 20:38:33 +0900 2025-07-14 15:47:26 +0900 online_resource text unknown unknown "" "" 981 https://hdl.handle.net/20.500.11932/94944 Guest "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" 104425 web web 2025-07-14 15:02:28 +0900 2025-07-14 15:47:26 +0900 105317 A Novel Boron-rich Scandium Borocarbosilicide; Sc0.83−xB10.0−yC0.17+ySi0.083−z (x=0.030, y=0.36 and z=0.026): Floating Zone Crystal Growth and Structure Analysis "" "" "" 2002-04-26 00:00:00 +0900 2002-04-26 2002 2015-12-15 20:34:47 +0900 2025-07-14 15:47:26 +0900 online_resource text unknown unknown "" "" 148 158 https://hdl.handle.net/20.500.11932/458054 Guest Single crystals of a novel boron-rich scandium borocarbosilicide Sc0.83−xB10.0−yC0.17+ySi0.083−z were grown by the floating zone method using a four-xenon lamp mirror-type image furnace. Structure analysis using single-crystal X-ray diffraction data showed that Sc0.83−xB10.0−yC0.17+ySi0.083−z has a face-centered cubic with lattice constant a=2.03085 nm and space group of F 3m. The crystal composition calculated from the structure analysis was ScB12.0C0.65Si0.071 which agreed with the measured composition of ScB12.7C0.62Si0.08. In the crystal structure which is a new structure type of boron-rich borides, there are three structurally independent B12 icosahedra I(1), I(2) and I(3) and one B10 polyhedron which interconnect each other to form a three-dimensional boron framework. There are four fully occupied bridging sites, one is the C site and the other three sites are occupied statistically by B or C. The Sc atoms reside in three interstitial sites of the boron framework. Two Si sites are tetrahedrally surrounded by the bridging carbon sites and by the bridging boron/carbon mixed occupation sites, respectively. The boron framework structure can be understood more easily by introducing larger structure units, they are a super tetrahedra T(1) made up by four icosahedra I(1), a super tetrahedra T(2) made up by four icosahedra I(2) and a super octahedra O(1) made up by six icosahedra I(3). "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" "" Sc0.83−xB10.0−yC0.17+ySi0.083−z; boron-rich scandium borocarbosilicide; floating zone crystal growth; single-crystal structure analysis; face-centered cubic structure; B10 polyhedron; B12 icosahedron//Sc0.83−xB10.0−yC0.17+ySi0.083−z; boron-rich scandium borocarbosilicide; floating zone crystal growth; single-crystal structure analysis; face-centered cubic structure; B10 polyhedron; B12 icosahedron//Sc0.83−xB10.0−yC0.17+ySi0.083−z; boron-rich scandium borocarbosilicide; floating zone crystal growth; single-crystal structure analysis; face-centered cubic structure; B10 polyhedron; B12 icosahedron "" "" "" "" 104424 web web 2025-07-14 15:02:28 +0900 2025-07-14 15:47:26 +0900